Retsch Cryomill Uživatelský manuál

© Retsch GmbH, 42781 Haan, Retsch-Allee 1-5, Germany 13.03.2013 0002 Manual Mixer Mill CryoMill Translation

Confirmation 10 Pos: 3.2 /00020 BD A Software/2 0005 PMGC Ka pitelsammlung/Ü berschrifte n/1. Überschrifte n/1 Bestätigu ng (Formular für den Betr

Technical data 11 Pos: 4.2 /00005 Üb erschriften/1. Üb erschriften/1 Technische Date n @ 0\ mod_1222344525 522_9.doc @ 2407 @ 1 @ 1 3 Technica

Technical data 12 CAUTION Hearing loss A high sound level may occur depending on the type of material, the number of balls used, the set grinding

Transport, scope of delivery, installation 13 Pos: 5.2 /00005 Üb erschriften/1. Üb erschriften/1 Verpackung, Tra nsport und Auf stellung @ 0\ mod_

Transport, scope of delivery, installation 14 NOTICE Atmospheric humidity – Electronic and mechanical components may be damaged and the performan

Transport, scope of delivery, installation 15 Fig. 1: Removing the transport bracket • Remove the screw (TA) using an Allen key. Fig. 2: • Pull

Transport, scope of delivery, installation 16 Fig. 3: Pulling out the condensation collecting filter • Pull the condensation collecting filter (R

Transport, scope of delivery, installation 17 The transport lock (TS), which is labelled with an arrow, is situated on the underneath of the devic

Transport, scope of delivery, installation 18 Fig. 7: Grip A grip (GL) is situated underneath both sides of the device • Use

Transport, scope of delivery, installation 19 11 Capacity 12 Amperage 13 Number of fuses 14 Fuse type and fuse strength In the case of ques

2 Copyright © Copyright by Retsch GmbH Haan, Retsch-Allee 1-5 D-42781 Haan Federal Republic of Germany

Transport, scope of delivery, installation 20 CAUTION Blocked pipe Ice formation – Ice or impurities can block pipes and thereby cause malfuncti

Transport, scope of delivery, installation 21 Fig. 9: Cooling jacket seal Pos: 5.33 /00010 Bedienungsa nleitungen Kapitels ammlungen

Transport, scope of delivery, installation 22 Fig. 11: Diagram of the cooling system Fig. 12: LED displays The temperature sensor (TSD) in the

Transport, scope of delivery, installation 23 CAUTION Risk of injury and danger of frostbite Bursting of the inlet hose. – Depending on the oper

Transport, scope of delivery, installation 24 Abb. 14: pressure relief • Press the (B10) pre-cooling and (B13) START keys simultaneously for 2

Transport, scope of delivery, installation 25 Fig. 16: Exhaust hose • Fasten the exhaust hose (BR) with the clamp (BS) to the outlet (B). – Th

Operating the machine 26 Pos: 6.2 /00005 Üb erschriften/1. Üb erschriften/1 Bedienung des Gerätes @ 0\ mod_1226565 880211_9.doc @ 3519 @ 1 @ 1

Operating the machine 27 Pos: 6.8 /00005 Üb erschriften/1.1 Ü berschrifte n/1.1 Überschrift en BDA/11 Gr afische Ansicht en der Bedienele mente und

Operating the machine 28 Fig. 18: Rear view 5.3 Summary table of device parts Element Description Function A Display and control unit: See below

Operating the machine 29 Pos: 6.11 /00005 Ü berschriften/ 1.1 Überschrifte n/1.1 Überschrift en BDA/11 Be dienelemente u nd Anzeigen @ 0\mod_122 6

3 1 Notes on the Operating Manual ... 6 1.

Operating the machine 30 Time plus button In setting mode and in operating mode: Increasing the set • Precooling • Grinding time • Intermediate

Operating the machine 31 Pos: 6.14 /00005 Ü berschriften/ 1.1 Überschrifte n/1.1 Überschrift en BDA/11 Ma hlbehälter einset zen @ 0\ mod_1226569844

Operating the machine 32 Fig. 20: Dismantling the grinding jar retaining device • Unscrew the lock nut (KM). • Remove the screw (SM). Fig. 21

Operating the machine 33 Fig. 22: Securing the grinding jar • First tighten the screw (SM) by hand (hand-tight). • Then tighten the lock nut a

Operating the machine 34 Fig. 23: Using the opening aid Pos: 6.20 /00004 Warnhinweis e/H0056 HINW EIS Cryomill PTFE Mahlbecher n ur mit Zimmert

Operating the machine 35 Fig. 24: Inserting the cooling jacket seal Pos: 6.23 /00005 Ü berschriften/ 1.1.1 Überschrift en/111 Adapter für 4/2 x

Operating the machine 36 Fig. 27: Inserting the grinding jar adapter Pos: 6.25 /00005 Ü berschriften/ 1.1.1 Überschrift en/111 Adapter für 4/2 x

Operating the machine 37 Note the positioning of the Eppendorf reaction vials. If you are using two or four reaction vials, these must be inserted

Operating the machine 38 Vkz + Mz = total grinding time Fig. 30: Sequence of a single grinding cycle Multiple grinding cycles consist of the preco

Operating the machine 39 The display advances one program each time the button is pressed - - > P1 > P2 > P3 > P4 > P5 > P6 >

4 5.7 Programs ...

Operating the machine 40 • Set the parameters for grinding as described in the following chapters: - Number of grinding cycles - Precooling - Grin

Operating the machine 41 – The first cycle consists of the precooling phase and grinding time – Cycles 2 to 9 each comprise an intermediate cool

Operating the machine 42 – The auto precooling (ap) LED is lit up. – “Auto” is shown in the time min display. Switch automatic precooling off •

Operating the machine 43 • Press the button (B12) to set the intermediate cooling . The intermediate cooling time LED lights up. • Use the buttons

Operating the machine 44 Fig. 40: Starting the grinding process • Press the START button to start the grinding process. – The Start LED (green)

Operating the machine 45 Fig. 43: Ending the grinding process • Press the STOP button to end the grinding process. The STOP LED (red) lights up.

Operating the machine 46 Fig. 45: Display of the operating hours The total operating time in hours is displayed. The maximum value that can be d

Operating the machine 47 Fig. 48: Replacing the device fuses The following glass fuses are needed for the CryoMill: 2 T4A • Pull the mains plu

Working instructions 48 Pos: 7.2 /00005 Üb erschriften/1. Üb erschriften/1 Arbeitsweis e @ 0\mod_12 26910058402 _9.doc @ 3661 @ @ 1 6 Working

Working instructions 49 Grinding jar nominal volume Sample quantity Max. feed size Ø7 mm Ø10 mm Ø12 mm Ø15 mm Ø20 mm Ø25 mm 5.0 ml 0.5 - 2.0 ml 2 mm

5 9.3.1 Dangers ...

Safety functions and fault display 50 Pos: 8.2 /00005 Üb erschriften/1. Üb erschriften/1 Sicherheitsfunktio nen und F ehleranzeige @ 0 \mod_1226 9

Cleaning, wear and service 51 Pos: 9.2 /00005 Üb erschriften/1. Üb erschriften/1 Reinigung, Versc hleiß und Wartung @ 0\ mod_12289899 74062_9.doc

Safety and occupational health instructions 52 The grinding tools may become worn, depending on the frequency of the grinding operation and the samp

Safety and occupational health instructions 53 nitrogen: oxygen deficiency situations, cryogenic burns, danger of explosion, oxygen enrichment • Al

Safety and occupational health instructions 54 Pos: 10.7 /00005 Ü berschriften/ 1.1 Überschrifte n/1.1 Überschrift en Dewar/11 De war Sicherheits h

Safety and occupational health instructions 55 • may not be transported in vehicles in filled state. • must be protected from impact, knocks and r

Safety and occupational health instructions 56 9.4.2.2 Burns through contact Contact of the skin with cold material causes frostbite or cryogenic

Safety and occupational health instructions 57 This list is not complete. Pos: 10.33 /0000 5 Überschriften/1 .1.1 Übersc hriften/111 Dewar Empfehl

Safety and occupational health instructions 58 • Remove all sources of fire (naked flame and light, spark producers, matches, lighters etc.). • Ve

Disposal 59 Pos: 11.2 /00005 Ü berschriften/ 1. Überschriften/ 1 Entsorgung @ 0\mod_12 34258746831 _9.doc @ 6173 @ @ 1 10 Disposal Pos: 11.3 /

Notes on the Operating Manual 6 Pos: 1.1 /00005 Üb erschriften/1. Üb erschriften/1 Hinweise zur B edienungsanlei tung @ 0\mo d_122234741 5287_9.do

60 11 Index4 4 A ... 47 5 5ml grinding jar position ...

61 Function of the hood switch ... 52 Fuse holder ... 47 Fuse stre

62 Power version ... 18 Precooling ... 41 P

63 V vapour plume ... 14 Version of the operating software ... 46 Voluminous m

Authorized person for the compilation of technical documents: J. Bunke (technical documentation) The following records are held by Retsch GmbH in

Copyright ® Copyright by Retsch GmbH Haan, Retsch-Allee 1-5 D-42781 Haan Federal Republic of Germany

Notes on the Operating Manual 7 Pos: 2.2 /00005 Üb erschriften/1.1 Ü berschrifte n/1.1 Überschrift en BDA/11 Er klärungen zu d en Sicherheits warnu

Notes on the Operating Manual 8 Pos: 2.5 /00005 Üb erschriften/1.1 Ü berschriften/ 1.1 Überschrifte n BDA/11 Gener elle Sicherhei tshinweise @ 0 \m

Notes on the Operating Manual 9 Pos: 2.11 /00005 Ü berschriften/ 1.1 Überschrifte n/1.1 Überschrift en BDA/11 Rep araturen @ 0\ mod_12236 24336511_